HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione → 1-Butanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione | HCID 260563 | — |
| Reactant | 3-Phenoxypyrrolidine | HCID 14497352 | — |
| Product | 1-Butanol | HCID 263 | 72% |
| Product | 2,4-dimethyl-6-(3-phenoxy-pyrrolidin-1-yl)-2H-[1,2,4]triazine-3,5-dione | HCID 58269788 | — |
Reaction Steps
The compound 38 (solid) is prepared from the triazine 1b and from the intermediate 11b according to the synthesis method 1 in n-butanol (yield: 72%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618287B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-e7ac4286367a47408cfcc6e734658efb |
| Source note | uspto-grants-2013_12 |