HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2,5-Dichlorophenoxy)piperidine → 4-(2-Chlorophenoxy)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2,5-Dichlorophenoxy)piperidine | HCID 16731696 | — |
| Reactant | 6-bromo-2-methyl-2H-[1,2,4]triazine-3,5-dione | HCID 58269813 | — |
| Product | 4-(2-Chlorophenoxy)piperidine | HCID 3864656 | — |
| Product | 6-(4-(2,5-dichlorophenoxy)piperidin-1-yl)-2-methyl-1,2,4-triazine-3,5(2H, 4H)-dione | HCID 58269798 | — |
Reaction Steps
The compound 91 (white solid) is prepared from the triazine 2e and from 4-(2,5-dichlorophenoxy)piperidine (obtained as under the preparative methods of intermediate 8a) according to the synthesis method 1 in toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618287B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-6c04e01d360d4ec2b1661f9c01e573ec |
| Source note | uspto-grants-2013_12 |