HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1917598Generated: November 2, 2026
p-Chlorophenacyl bromide → HCID 86659071, compound
https://huagongshe.com/reaction/1917598
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | p-Chlorophenacyl bromide | HCID 68303 | — |
| Reactant | 4-Isopropylpyridine | HCID 69674 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86659071 | HCID 86659071 | 78% |
Reaction Steps
To a solution of 4-isopropylpyridine (3.12 g, 25.7 mmol) in acetonitrile (25 mL) is added 2-bromo-4′-chloro-acetophenone (6.01 g, 25.7 mmol). The mixture is stirred at 23° C. overnight then the resulting precipitate is filtered, collected, and dried to afford the title intermediate (7.10 g, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08618300B2 |
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| Source dataset | uspto-grants-2013_12 |
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| ORD ID | ord-a6e9c2cd01284b138aecab870f1b0c3d |
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| Source note | uspto-grants-2013_12 |
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