HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(6-Nitropyridin-3-yl)morpholine → 5-Morpholinopyridin-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(6-Nitropyridin-3-yl)morpholine | HCID 2927973 | — |
| Reactant | tert-Butyl 4-(6-aminopyridin-3-yl)piperazine-1-carboxylate | HCID 11737525 | — |
| Product | 5-Morpholinopyridin-2-amine | HCID 11367346 | — |
Reaction Steps
Following the procedures as described for 188b and starting with 1 g of 4-(6-nitropyridin-3-yl)morpholine, 255b was obtained as a yellow solid (840 mg, 98%). MS: [M+H]+ 210
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618107B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-0a127c7091ac4e5aa569bd675096cb9b |
| Source note | uspto-grants-2013_12 |