反应详情

温度

25 °C

A 250-mL single-neck round-bottomed flask equipped with a magnetic stirrer was charged with 336c (3.0 g, 13.5 mmol), methanol (80 mL), and Pd/C (10%) (300 mg). The reaction mixture was stirred at 25° C. under H2 for 15 h. After the reaction was finished, it was filtered and concentrated to afford 336d as a yellow oil (1.6 g, 90%).

1. customA 250-mL single-neck round-bottomed flask equipped with a magnetic stirrer
2. filtrationit was filtered
3. concentrationconcentrated