HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azane;hydrate → 2-Methylthiazole-5-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azane;hydrate | HCID 12896473 | — |
| Reactant | Methyl 2-methyl-1,3-thiazole-5-carboxylate | HCID 21427465 | — |
| Product | 2-Methylthiazole-5-carboxamide | HCID 23322366 | 73% |
Reaction Steps
1.4 g Methyl 2-methylthiazol-5-carboxylate was added to 25 ml ammonia water, to carry out reaction at room temperature for 3 hr. The reaction product was cooled down, filtered, and washed with water to obtain 0.95 g a white powdery solid (73%) with mp 202-205 (C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168642B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-c38b706d80a24896bfb56f94447db64e |
| Source note | uspto-grants-2012_05 |