HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 20544504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-Aminothiazole-5-carbonitrile | HCID 10057507 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20544504 | HCID 20544504 | 80% |
Reaction Steps
2.14 g 2-Amino-5-cyanothiazole was dissolved in 10 ml acetic acid, and 1.8 ml acetic anhydride was added to carry out reaction at 100° C. for 30 min. The reaction product was cooled down, and filtered to obtain 2.5 g of a clay-solid having metallic luster (yield 80%), 1H NMR (DMSO-d6) 2.22 (3H, s), 8.36 (1H, s), 12.95 (1H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168642B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-47e75d2f864c491e925dee59704ce60e |
| Source note | uspto-grants-2012_05 |