HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59235234, compound → HCID 59235235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59235234 | HCID 59235234 | — |
| Solvent | Ethanol hydrochloride | HCID 21887872 | — |
| Product | HCID 59235235 | HCID 59235235 | 88% |
Reaction Steps
500 mg 4-[1-(3,4-dichlorophenyl)-2,5-dioxo-4-(4-hydroxyphenyl)-4-methylimidazolidin-3-yl]-2-butynyl acetate (the product of Example 223) are dissolved in 10 mL of a 2 N ethanol/HCl mixture (70/30). The mixture is stirred under reflux for 3 hours then concentrated and dried under vacuum. 400 mg of a white solid are obtained (Yd=99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168667B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-4788b1c6dd664d278978d737a3a6847e |
| Source note | uspto-grants-2012_05 |