HRID1919836

反应详情

EQUATION

反应方程式

HRID 1919836 的结构方程式

PROCEDURE

实验过程

The title compound was synthesized according to the procedure described for the synthesis of [1-(6-tert-butylpyridin-3-yl)ethyl]amine starting from 6-tert-butyl-2-methoxynicotinonitrile (intermediate 23) (66 mg, 0.347 mmol), MeMgBr 1.4 M 75/25 toluene/THF (743 μL, 1.04 mmol) and NaBH4 (32.8 mg, 0.87 mmol Material isolated from the workup was used without further purification in the preparation.

WORKUP

后处理

  1. customisolated from the workup
  2. customwas used without further purification in the preparation