1,4-Dioxane hydrochloride → HCID 67496791, compound

Participants

Reaction Steps

tert-Butyl 4-{2-anilino-1-[(dimethylamino)methyl]-2-oxoethyl}benzoate (350 mg, 0.95 mmol) was taken up in 4 M HCl/dioxane (10 mL) and stirred at room temperature for 16 h. The solution was concentrated to dryness to give 4-{2-anilino-1-[(dimethylamino)methyl]-2-oxoethyl}benzoic acid hydrochloride as a white, flaky solid. MS (ESI) calcd [M+H]+ 313.1, found 313.1.

Provenance & Evidence