HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 59157922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | HCID 59157961 | HCID 59157961 | — |
| Product | HCID 59157922 | HCID 59157922 | — |
Reaction Steps
To 1-bromo-6-(bromomethyl)-2-iodonaphthalene (270 mg) from step 4 was added triethylphosphite (4 mL). The reaction mixture was heated at reflux for 1 hour followed by removal of excess triethylphosphite under high vacuum distillation yielding the titled product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168815B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-ce7959ef63484b9485285dfba18a4c4a |
| Source note | uspto-grants-2012_05 |