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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1920564Generated: October 30, 2026

HCID 67496327, compound → HCID 67496802, compound

https://huagongshe.com/reaction/1920564

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67496327HCID 67496327—
CatalystPalladiumHCID 23938—
SolventDimethylformamideHCID 6228—
ProductHCID 67496802HCID 67496802—

Reaction Steps

To a solution of (R)-1-[2-(4-Benzyloxy-benzoylamino)-ethyl]-3-(2-hydroxy-2,2-diphenyl-acetoxy)-1-azonia-bicyclo[2.2.2]octane bromide (0.075 g, 0.11 mmol) in DMF (1 ml) under an argon atmosphere is added 10% Pd on carbon (40 mg) and the resulting solution hydrogenated for 3 hours. The catalyst is then removed by filtration and concentration in vacuo yields the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08168654B2
Source datasetuspto-grants-2012_05
ORD IDord-4f90aa2f6ede465c86aa26170362b57a
Source noteuspto-grants-2012_05