HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67496327, compound → HCID 67496802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67496327 | HCID 67496327 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67496802 | HCID 67496802 | — |
Reaction Steps
To a solution of (R)-1-[2-(4-Benzyloxy-benzoylamino)-ethyl]-3-(2-hydroxy-2,2-diphenyl-acetoxy)-1-azonia-bicyclo[2.2.2]octane bromide (0.075 g, 0.11 mmol) in DMF (1 ml) under an argon atmosphere is added 10% Pd on carbon (40 mg) and the resulting solution hydrogenated for 3 hours. The catalyst is then removed by filtration and concentration in vacuo yields the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168654B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-4f90aa2f6ede465c86aa26170362b57a |
| Source note | uspto-grants-2012_05 |