HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 16662203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 3-Chloro-6-phenylpyridazine | HCID 88515 | — |
| Reactant | 9-Boc-3,9-diaza-bicyclo[3.3.1]nonane | HCID 54595539 | — |
| Product | HCID 16662203 | HCID 16662203 | — |
Reaction Steps
Was prepared according to reaction-conditions of Method A from 9-tert-butoxycarbonyl-3,9-diazabicyclo[3.3.1]nonane and 3-chloro-6-phenylpyridazine at 130° C. for 3 days, followed by treatment with TFA. Workup procedure was done according to Method A. LC-ESI-HRMS of [M+H]+ shows 281.1761 Da. Calc. 281.176621 Da, dev. −1.9 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173658B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-6cc36df180d34ede8071dd02eaf4ed03 |
| Source note | uspto-grants-2012_05 |