HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2,4-Difluorobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2,4-Difluorobenzoyl chloride | HCID 588081 | — |
| Product | Methyl 2,4-Difluorobenzoate | HCID 2782897 | — |
Reaction Steps
To 100 mL of MeOH, 2,4-difluorobenzoyl chloride (10 mL, 79.3 mmol) was added and the mixture stiffed at room temperature for 2 hours. The solvent was then evaporated affording the title compound as pale yellow oil (quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173659B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-86bd4f34dbc14c0db9e171f11e8e1de9 |
| Source note | uspto-grants-2012_05 |