HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 18449380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 86607785 | HCID 86607785 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 18449380 | HCID 18449380 | — |
Reaction Steps
(±)-tert-Butyl {3-[4-(methylsulfinyl)-1,3-thiazol-2-yl]-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl}acetate from Step D (100 mg, 0.254 mmol) was dissolved in CF3CO2H (3 mL) and CH2Cl2 (3 mL) and the mixture was stirred at ambient temperature for 3 h, then concentrated in vacuo to give the title compound. MS: m/z=338 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173655B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-e1df370f8b0a45b6b58caf8c33af93bb |
| Source note | uspto-grants-2012_05 |