Methylhydrazine → HCID 23117145, compound

HRID 1921259Notes

Reaction equation

HRID 1921259 reaction equation
[CH:1]1([C:7]([C:9]2[CH:14]=[CH:13][C:12]([O:15][CH2:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[CH:11][C:10]=2F)=O)[CH2:6][CH2:5][CH2:4][CH2:3]C1.[OH2:24].NN.[CH3:27][NH:28][NH2:29].[CH2:30](NN)[C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1>>[CH2:16]([O:15][C:12]1[CH:11]=[C:10]2[C:9]([C:7]([CH:1]3[CH2:3][CH2:4][CH2:5][CH2:6]3)=[N:29][N:28]2[C:27]2[CH:9]=[CH:7][C:1]([O:24][CH2:30][C:31]3[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=3)=[CH:6][CH:5]=2)=[CH:14][CH:13]=1)[C:17]1[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=1

Participants

5

Reactant 4

HCID 6061MethylhydrazineHCID 11157(Phenylmethyl)hydrazineHCID 24654Hydrazine hydrate (1:1)HCID 67219586HCID 67219586, compound

Product 1

HCID 23117145HCID 23117145, compound

Procedure

Using the same procedure but replacing cyclopentyl (4-benzyloxy-2-fluorophenyl)methanone by cyclohexyl (4-benzyloxy-2-fluorophenyl)methanone and hydrazine hydrate by methylhydrazine or benzylhydrazine, the following compound were respectively obtained:

Workup

  1. customthe following compound were respectively obtained

Sources & evidence

ORD record
ord-25e32b7a57c1430bba0f9f18c202b126
Source dataset
uspto-grants-2012_05
Patent number
US08173679B2

Reaction notes

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