HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58413020, compound → HCID 71083020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58413020 | HCID 58413020 | — |
| Reactant | 5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)thiophene-2-sulfonyl chloride | HCID 86610352 | — |
| Product | HCID 71083020 | HCID 71083020 | 39% |
Reaction Steps
5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)thiophene-2-sulfonyl chloride is reacted with [3-(3,3-difluoro-pyrrolidin-1-yl)-propyl]-amine as described in Step 5, Example 24 to give the title compound (39% yield). LC/MS: RT 1.69 min; m/e=446 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-86b66cc694dd4340adb6463a2c9263e0 |
| Source note | uspto-grants-2012_05 |