2-(Pyridin-3-yl)ethan-1-amine → HCID 71083006, compound

Participants

Reaction Steps

5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-sulfonyl chloride is reacted with (2-pyridin-3-yl)ethylamine as described in Step 5, Example 24 to give the title compound as a solid (34% yield). LC/MS: RT 2.00 min; m/e 388 (M+H); 1H NMR (δ, ppm): 8.75 (2H), 7.90-8.36 (3H), 7.45 (1H, s), 7.13 (1H, d); 6.68 (1H, d), 3.27 (2H), 2.96 (2H), 2.36 (3H, s), 2.40 (2H), 1.11 (3H, t).

Provenance & Evidence