1-Methylhomopiperazine → HCID 67492162, compound

Participants

Reaction Steps

5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-sulfonyl chloride is reacted with 1-methyl-1,4-diazepane as described in Steps 5 and 6, Example 1 to give the title compound as a solid (73% yield). LC/MS: RT 2.00 min; m/e 380 (M+H); 1H NMR (CDCl3, δ, ppm): 11.81 (1H), 7.51 (1H), 7.29 (1H), 6.78 (1H); 3.85 (2H), 3.46 (6H), 3.19 (2H), 2.78 (3H), 2.40 (5H), 1.09 (3H, t).

Provenance & Evidence