HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[(1-Ethyl-pyrrolidin-2-ylmethyl)-amino]-propyl amine → HCID 58808542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[(1-Ethyl-pyrrolidin-2-ylmethyl)-amino]-propyl amine | HCID 67492365 | — |
| Reactant | 5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)thiophene-2-sulfonyl chloride | HCID 86610352 | — |
| Product | HCID 58808542 | HCID 58808542 | 19% |
Reaction Steps
5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)thiophene-2-sulfonyl chloride is reacted with 3-[(1-ethyl-pyrrolidin-2-ylmethyl)-amino]-propyl amine as described in Step 5, Example 24 to give the title compound (19% yield). LC/MS: RT 2.19 min; m/e 467 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-d49031b62e674c31b74a6a34abe891d1 |
| Source note | uspto-grants-2012_05 |