HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 63653380, compound → HCID 58808602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 63653380 | HCID 63653380 | — |
| Reactant | 5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)thiophene-2-sulfonyl chloride | HCID 86610352 | — |
| Product | HCID 58808602 | HCID 58808602 | 88% |
Reaction Steps
5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)thiophene-2-sulfonyl chloride is reacted with 1-(2-aminoethyl)-pyrrolidine-2-carboxylic acid as described in Step 5, Example 24 to give the title compound (88% yield). LC/MS: RT 2.04 min; m/e 440 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-cdbe3aea4f3b4f20a7d13dbc62f65494 |
| Source note | uspto-grants-2012_05 |