HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Cyclopropylcarbonyl)piperazine → 5'-(4-Cyclopropanecarbonyl-piperazine-1-carbonyl)-5-ethyl-2-methyl-1H-[3,3']bipyridinyl-6-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Cyclopropylcarbonyl)piperazine | HCID 2064235 | — |
| Reactant | 5'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid | HCID 58808702 | — |
| Product | 5'-(4-Cyclopropanecarbonyl-piperazine-1-carbonyl)-5-ethyl-2-methyl-1H-[3,3']bipyridinyl-6-one | HCID 58808695 | — |
Reaction Steps
Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[3,3′]bipyridinyl-5-carboxylic acid and 4-cyclopropanecarbonyl-piperazine to afford the title compound. MS: m/e=395 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-d3ec8d9c5c0b48eb8a9ce8eca32997c5 |
| Source note | uspto-grants-2012_05 |