HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,O-Dimethylhydroxylamine → HCID 58808530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,O-Dimethylhydroxylamine | HCID 14232 | — |
| Reactant | HCID 67492337 | HCID 67492337 | — |
| Product | HCID 58808530 | HCID 58808530 | 85% |
Reaction Steps
Method 1, Example 205 is substantially repeated except for utilizing 5-(5-ethyl-2-methyl-6-oxo-1,6-dihydro-pyridin-3-yl)-thiophene-2-carboxylic acid and methoxy-methylamine to afford the title compound (85% yield). LC/MS: RT 2.64 min; m/e 307 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-f6c93336849e4b0e9430f6a53d951f47 |
| Source note | uspto-grants-2012_05 |