HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylethylenediamine → HCID 57608795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylethylenediamine | HCID 66053 | — |
| Reactant | ethyl N-carbonylcarbamate | HCID 300166 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 57608795 | HCID 57608795 | — |
Reaction Steps
A solution of ethyl isocyanatoformate (500 mg, 4.2 mmol) in absolute diethyl ether (15 mL) was added dropwise to a solution of N1.N1-dimethylethane-1,2-diamine (440 mg, 550 μL, 5 mmol) in diethyl ether (25 mL) and stirred for 2 h at room temperature. The precipitate was filtered off and the filtrate was concentrated under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173700B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-17a25549d99040cea0c8c737aa281441 |
| Source note | uspto-grants-2012_05 |