HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 86643648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 69108330 | HCID 69108330 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86643648 | HCID 86643648 | — |
Reaction Steps
7.77 g (21 mmol) of 9H-fluoren-9-ylmethyl (4-acetylcyclohexyl)carbamate (cis compound) is dissolved in 100 mL of methanol at ambient temperature and combined with 1.09 mL (21 mmol) of bromine. The mixture is stirred for 16 hours at ambient temperature, cooled, and the crystals precipitated are suction filtered. Yield: 6.35 g (50%); NMR: LG201641.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173699B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-6a01e464f6334b8ebfa61202c804c20a |
| Source note | uspto-grants-2012_05 |