HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 59305817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 86643647 | HCID 86643647 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59305817 | HCID 59305817 | — |
Reaction Steps
1.10 g (2 mmol) of 9H-fluoren-9-ylmethyl[4-(2-methylthiazol-4-yl)cyclohexyl]carbamate (cis compound) and 15 mL of diethylamine are stirred in 30 mL of THF for 16 hours at ambient temperature. Then the reaction mixture is concentrated by evaporation and the residue is combined with THF and concentrated again by evaporation. The residue is purified by chromatography. Yield: 0.13 g (36%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173699B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-a72f4a5dfb1b49efac082325a7284bc8 |
| Source note | uspto-grants-2012_05 |