Lithium hydroxide, monohydrate → HCID 57572049, compound

HRID 1921955Notes

Reaction equation

HRID 1921955 reaction equation
[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O:6]C)=[O:5].O.[OH-].[Li+:12]>CO.O>[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O-:6])=[O:5].[Li+:12]

Participants

5

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 19792887Methyl 2-methoxybutanoate

Product 1

HCID 57572049HCID 57572049, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

In a 15-mL RBF was dissolved methyl 2-methoxybutanoate (0.027 g, 0.20 mmol) in methanol (0.75 mL). A solution of lithium hydroxide monohydrate (0.0086 g, 0.20 mmol) in water (0.75 mL) was added, and the mixture was stirred overnight. The mixture was concentrated to afford the title compound.

Workup

  1. concentrationThe mixture was concentrated

Sources & evidence

ORD record
ord-aadbfe4a3c9e44f089f13c09a437ad3a
Source dataset
uspto-grants-2012_05
Patent number
US08173810B2

Reaction notes

Loading…