HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20033286, compound → HCID 20033363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20033286 | HCID 20033286 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20033363 | HCID 20033363 | 60% |
Reaction Steps
To a solution of 1-[2-(3-Nitro-phenyl)-ethyl]-piperidine in ethanol was added a catalytic amount 10% activated palladium on carbon and excess hydrogen gas. This mixture was allowed to stir overnight, then filtered and concentrated. The product was clean enough for the next reaction. 60% yield. MH+=205.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173689B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-c0b77b4c589e4856ba8d2c1008ba4aed |
| Source note | uspto-grants-2012_05 |