HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → (S)-N-(5-bromo-2,3-dihydro-1H-inden-2-yl)propane-2-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | (s)-5-Bromo-2-aminoindane camphorsulfonate salt | HCID 86650331 | — |
| Product | (S)-N-(5-bromo-2,3-dihydro-1H-inden-2-yl)propane-2-sulfonamide | HCID 46899974 | — |
Reaction Steps
N-[(2S)-5-bromo-2,3-dihydro-1H-inden-2-yl]-2-propanesulfonamide was prepared using a similar method to that disclosed in WO 2006/015828; the initial solvent for conversion of (S)-5-bromo-2-aminoindane camphorsulfonate salt into the free base form was DCM.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173820B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-b6da3761a99a4a3aa31ae4344bb8d355 |
| Source note | uspto-grants-2012_05 |