HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86635050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58005118 | HCID 58005118 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86635050 | HCID 86635050 | — |
Reaction Steps
Carbamate from Step 2 was dissolved in a 4.0 M HCl solution in dioxane. The resulting mixture was stirred at RT for 0.5 h, during which time the product precipitated. The title compound was filtered off and washed with hexane/EtOAc 1/1 v/v. MS (ES+) C17H18N2O3 requires 298. Found: 299 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178520B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-8c9af6f6062145a486a7b1057b343477 |
| Source note | uspto-grants-2012_05 |