HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 44549476, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 44550117 | HCID 44550117 | — |
| Product | HCID 44549476 | HCID 44549476 | — |
Reaction Steps
A 0.27 M solution of carbamate from Step 1 in 4N HCl/dioxane was stirred at RT for 2 h. The volatiles were then removed under reduced pressure to give the title compound as an off-white solid that was used directly in the next step. MS (ES+) C22H27N3O4 requires: 397. Found: 398 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178520B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-af658bcef1fa405f88d5a7ae7f2f3eae |
| Source note | uspto-grants-2012_05 |