Phenylhydrazine → HCID 46219191, compound

HRID 1924483Notes

Reaction equation

HRID 1924483 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][CH:15]=2)[N:8]=1)=O.[C:23]1([NH:29]N)[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[CH3:21][O:20][C:17]1[CH:18]=[CH:19][C:14]([N:9]2[CH:10]=[CH:11][C:12](=[O:13])[C:7]([C:5]3[N:29]([C:23]4[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=4)[N:2]=[CH:3][CH:4]=3)=[N:8]2)=[CH:15][CH:16]=1

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 59370008HCID 59370008, compound

Product 1

HCID 46219191HCID 46219191, compoundYield 81%

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-methoxyl-phenyl)-1H-pyridazin-4-one (A-2) and phenylhydrazine according to the method described for Example 1 in 81% yield. MS: M=345.0 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-7dca4af680b84374ba860067f616b903
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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