Hydrochloric Acid → HCID 46219818, compound

HRID 1924515Notes

Reaction equation

HRID 1924515 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:8]=1)=O.[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([NH:28]N)=[CH:24][CH:23]=1.Cl>>[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([N:28]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)=[CH:24][CH:23]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 70624(4-Chlorophenyl)hydrazineHCID 12742246(E)-3-(3-(Dimethylamino)acryloyl)-1-phenylpyridazin-4(1H)-one

Product 1

HCID 46219818HCID 46219818, compoundYield 51%

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-phenyl-1H-pyridazin-4-one (A-1) and 4-chloro-phenylhydrazine×HCl according to the method described for Example 1 in 51% yield.

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-bb08929c0dd2483f964408873a9572f1
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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