Hydrochloric Acid → HCID 59369994, compound

HRID 1924516Notes

Reaction equation

HRID 1924516 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:8]=1)=O.[C:21]1([CH3:29])[CH:26]=[CH:25][C:24]([NH:27]N)=[CH:23][CH:22]=1.Cl>>[C:14]1([N:9]2[CH:10]=[CH:11][C:12](=[O:13])[C:7]([C:5]3[N:27]([C:24]4[CH:25]=[CH:26][C:21]([CH3:29])=[CH:22][CH:23]=4)[N:2]=[CH:3][CH:4]=3)=[N:8]2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 10875(4-Methylphenyl)hydrazineHCID 12742246(E)-3-(3-(Dimethylamino)acryloyl)-1-phenylpyridazin-4(1H)-one

Product 1

HCID 59369994HCID 59369994, compoundYield 67%

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-phenyl-1H-pyridazin-4-one (A-1) and p-tolylhydrazine×HCl according to the method described for Example 1 in 67% yield.

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-efc3cb48f6544db88378607d7888c946
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

Loading…