3-Hydrazinopyridine → HCID 59370177, compound
Reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=2)[N:8]=1)=O.[N:26]1[CH:31]=[CH:30][CH:29]=[C:28]([NH:32][NH2:33])[CH:27]=1>>[N:26]1[CH:31]=[CH:30][CH:29]=[C:28]([N:32]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([O:20][C:21]([F:22])([F:23])[F:24])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:33]2)[CH:27]=1Participants
3
Procedure
The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-8) and pyridine-3-yl-hydrazine according to the method described for example 43. MS: M=400.1 (M+H)+
Workup
- customThe product was obtained
Sources & evidence
- ORD record
- ord-ecb0fb42c0664c78a500512c13f8d14d
- Source dataset
- uspto-grants-2012_05
- Patent number
- US08178538B2
Reaction notes
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