Phenylhydrazine → HCID 59370088, compound

HRID 1924680Notes

Reaction equation

HRID 1924680 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][CH:15]=2)[N:8]=1)=O.[C:25]1([NH:31][NH2:32])[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[C:25]1([N:31]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([C:20]([F:22])([F:21])[F:23])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:32]2)[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 5704110HCID 5704110, compound

Product 1

HCID 59370088HCID 59370088, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethyl-phenyl)-1H-pyridazin-4-one (A-22) and phenylhydrazine according to the method described for example 1. MS: M=383.2 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-13c0dc169f03469c9e24e0cc54db1719
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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