Phenylhydrazine → HCID 59369977, compound

HRID 1924724Notes

Reaction equation

HRID 1924724 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][CH2:21][C:22]([F:25])([F:24])[F:23])=[CH:16][CH:15]=2)[N:8]=1)=O.[C:27]1([NH:33][NH2:34])[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:27]1([N:33]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([O:20][CH2:21][C:22]([F:24])([F:23])[F:25])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:34]2)[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 59370013HCID 59370013, compound

Product 1

HCID 59369977HCID 59369977, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-[4-(2,2,2-trifluoro-ethoxy)-phenyl]-1H-pyridazin-4-one (A-32) and phenylhydrazine according to the method described for example 43. MS: M=413.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-30642b7a632043ffb0896041658b8ac4
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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