HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67519674, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59448375 | HCID 59448375 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67519674 | HCID 67519674 | — |
Reaction Steps
2,4-bis(methyloxy)-5-(1,3-thiazol-2-yl)pyrimidine (Prep25, 294 mg, 1.225 mmol) was suspended in 4M HCl solution in 1,4-dioxane (25 ml) to give a white suspension. After 1 h at 90° C., the solvent was evaporated. 306.8 mg of the title compound were isolated as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178549B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-4691cde53b2d466da4147012d47aac93 |
| Source note | uspto-grants-2012_05 |