HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67519619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 25252825 | HCID 25252825 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67519619 | HCID 67519619 | 91.2% |
Reaction Steps
5-(1-methyl-1H-pyrrol-2-yl)-1-(3-{(1S,5R)-1-[4-(trifluoromethyl)phenyl]-3-azabicyclo[3.1.0]hex-3-yl}propyl)-2,4(1H,3H)-pyrimidinedione (18.1 mg, 0.039 mmol) was suspended in Diethyl ether (1 ml) and Hydrochloric acid (0.047 ml, 0.047 mmol) 1M in Et2O was added. A suspension was formed that was dried (vacuo). The white solid formed was triturated with Et2O (3×0.3 mL) to afford the title compound as a white solid (17.6 mg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178549B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-14e780b175454910882989f81dc6f60c |
| Source note | uspto-grants-2012_05 |