HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67519771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 25253293 | HCID 25253293 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67519771 | HCID 67519771 | — |
Reaction Steps
5-(4-methyl-1H-pyrazol-1-yl)-1-(3-{(1S,5R)-1-[4-(trifluoromethyl)phenyl]-3-azabicyclo[3.1.0]hex-3-yl}propyl)-2,4(1H,3H)-pyrimidinedione (E31, 4.8 mg, 9.92 μmol) was dissolved and sonicated in Diethyl ether (1 ml) to give a colorless solution. 1.0 M solution of HCl in Diethyl ether (0.025 ml, 0.025 mmol) was added at room temperature. After 3 min the solvent was evaporated to obtain 5.3 mg of the title compound as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178549B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-8353a40e130741f498a5a760d3b3ad98 |
| Source note | uspto-grants-2012_05 |