huagongshe.com
HRID1925117

反应详情

EQUATION

反应方程式

HRID 1925117 的结构方程式

REACTANTS

反应物

2
结构：C1COCCO1.Cl
HCID20443148

1,4-Dioxane hydrochloride

C4H9ClO2

结构：CC(C)(C)OC(=O)Nc1cn2nc(Cn3nnc4ccc(Br)cc43)ccc2n1
HCID59233266

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Nc1cn2nc(Cn3nnc4ccc(Br)cc43)ccc2n1
HCID66633482

未命名化合物

PROCEDURE

实验过程

A solution of compound 10H (0.44 g, 1.0 mmol) in 4N HCl/dioxane (10 mL) was stirred at room temperature for 60 minutes, concentrated and dried in vacuum to give 0.3 g of product (10) as a hydrochloride salt. ESI-MS:m/z 344.1 (M+H)+.

WORKUP

后处理

  1. concentrationconcentrated
  2. customdried in vacuum