HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1925129Generated: October 28, 2026
Hydrazine hydrate (1:1) → 2-(6-Hydrazinylpyridin-3-yl)propan-2-ol
https://huagongshe.com/reaction/1925129
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2-(6-Chloropyridin-3-yl)propan-2-ol | HCID 12562118 | — |
| Product | 2-(6-Hydrazinylpyridin-3-yl)propan-2-ol | HCID 55281792 | — |
Reaction Steps
A mixture of 2-(6-chloropyridin-3-yl)propan-2-ol (975 mg, 5.68 mmol), and hydrazine hydrate (5512 μl, 114 mmol) was heated in a microwave on high absorbance for 10 hr at 110° C. The mixture was cooled to room temperature and the hydrazine was removed via rotary evaporation. The resulting yellow residue was used without further work-up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08178534B2 |
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| Source dataset | uspto-grants-2012_05 |
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| ORD ID | ord-27ccae116e6240efa30b94b759b11845 |
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| Source note | uspto-grants-2012_05 |
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