HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazinopyridine → HCID 59233223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazinopyridine | HCID 78645 | — |
| Reactant | HCID 59233190 | HCID 59233190 | — |
| Product | HCID 59233223 | HCID 59233223 | — |
Reaction Steps
The title compound was synthesized using an analogous procedure to that described in the preparation of Compound 48 (Method A) using 2-hydrazinylpyridine. 1H NMR (400 MHz, DMSO-d6) δ ppm 0.73-0.87 (m, 4 H) 1.83-1.99 (m, 4 H) 5.04-5.15 (m, 1 H) 6.94-7.04 (m, 1 H) 7.19 (d, J=9.35 Hz, 1 H) 7.38-7.47 (m, 1 H) 7.80 (d, J=9.35 Hz, 1 H) 7.94 (d, J=9.85 Hz, 1 H) 8.10 (s, 1 H) 8.35 (d, J=7.07 Hz, 1 H) 11.14 (s, 1 H). MS:m/z 348.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178534B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-0c6aec362b154cb2918b9bf3b9351db7 |
| Source note | uspto-grants-2012_05 |