HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl 6-hydroxy-2-naphthoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 6-Hydroxy-2-naphthoic acid | HCID 85557 | — |
| Product | Methyl 6-hydroxy-2-naphthoate | HCID 390995 | — |
Reaction Steps
Through a solution of 6-hydroxynaphthalene-2-carboxylic acid (4.87 g, 26 mmol, Aldrich) in MeOH (100 mL, Aldrich) was bubbled HCl gas for 1 h. The resulting mixture was stirred for 10 h at RT. The solution was concentrated in vacuo to give the title compound as a pink powder. MS (ESI, pos. ion) m/z: 203 (M+1). Mass Calc'd for C12H10O3: 202.06.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178557B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-413f0073e6714285b4d343b0e5365de8 |
| Source note | uspto-grants-2012_05 |