HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 24823893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 2,4-Dichloropyridine | HCID 33515 | — |
| Reactant | 6-Hydroxy-1-naphthoic acid | HCID 5463800 | — |
| Product | HCID 24823893 | HCID 24823893 | — |
Reaction Steps
6-hydroxy-1-napthoic acid (3.2 g, 17 mmol) was reacted with 2,4-dichloropyridine (2.5 g, 17 mmol) and Cs2CO3 (16.6 g, 51 mmol) under the conditions of Example 421 step a to furnish the title compound as a brown solid. MS (ESI, pos. ion) m/z: 300.4 (M+1). Mass Calc'd for C16H10ClNO3: 299.708.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178557B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-fbf7191d23734d70aa0821aed191129e |
| Source note | uspto-grants-2012_05 |