HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloropyridine-2-carboxamide → HCID 67520303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloropyridine-2-carboxamide | HCID 303543 | — |
| Reactant | 6-Hydroxy-1-naphthoic acid | HCID 5463800 | — |
| Product | HCID 67520303 | HCID 67520303 | — |
Reaction Steps
6-Hydroxy-1-napthoic acid (2.5 g, 13 mmol) was reacted with 4-chloropicolinamide (WO 02/085857) (2.6 g, 15 mmol) under the conditions of Example 421 Step a to give the title compound as a brown solid. MS (ESI, pos. ion) m/z: 309.2 (M+1). Mass Calc'd for C17H12N2O4: 308.29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178557B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-39463189ba40427e83a7fcbf675a3bf1 |
| Source note | uspto-grants-2012_05 |