HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86649161, compound → HCID 67520595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86649161 | HCID 86649161 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67520595 | HCID 67520595 | 87.3% |
Reaction Steps
Obtained from Intermediate 35 (1.3 g, 3.37 mmol) in hydrogen chloride 1.25M in methanol by the same procedure described in Intermediate 17. The precipitate obtained was separated by filtration giving the title compound as a yellow solid (0.84 g, 87%). MS (M+): 286.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178679B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-6fa4c6590e31404b9d94ef4d00673872 |
| Source note | uspto-grants-2012_05 |