HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67520709, compound → HCID 42623781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67520709 | HCID 67520709 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 42623781 | HCID 42623781 | 69% |
Reaction Steps
Obtained from Intermediate 38 (0.17 g, 0.32 mmol) and palladium on charcoal (10%, 0.034 g) by the same procedure described in Example 1 (reaction time: 2 days). The crude obtained was triturated with ether and filtrated to obtain the title compound as a yellow solid (0.102 g, 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178679B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-1f68c221155c45488ee5089b71d9cbe9 |
| Source note | uspto-grants-2012_05 |