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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1925514Generated: November 1, 2026

HCID 86649163, compound → HCID 67520775, compound

https://huagongshe.com/reaction/1925514

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86649163HCID 86649163—
SolventHydrochloric AcidHCID 313—
SolventMethanolHCID 887—
ProductHCID 67520775HCID 67520775—

Reaction Steps

Obtained from Intermediate 50 (1.2 g, 2.94 mmol) in hydrogen chloride 1.25 M in methanol by the same procedure described in Intermediate 17. The solvent was removed under reduced pressure and the title compound was obtained as a salt (0.62 g, 67%), which was used in the next step without further purification. MS (M+): 314.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08178679B2
Source datasetuspto-grants-2012_05
ORD IDord-133557197f304ed98c3047a824e850a8
Source noteuspto-grants-2012_05