HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86649163, compound → HCID 67520775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86649163 | HCID 86649163 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67520775 | HCID 67520775 | — |
Reaction Steps
Obtained from Intermediate 50 (1.2 g, 2.94 mmol) in hydrogen chloride 1.25 M in methanol by the same procedure described in Intermediate 17. The solvent was removed under reduced pressure and the title compound was obtained as a salt (0.62 g, 67%), which was used in the next step without further purification. MS (M+): 314.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178679B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-133557197f304ed98c3047a824e850a8 |
| Source note | uspto-grants-2012_05 |