HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67520630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86649168 | HCID 86649168 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67520630 | HCID 67520630 | — |
Reaction Steps
Obtained from Intermediate 79 (1.25 g, 3.13 mmol) and hydrogen chloride 1.25 M in methanol (40 mL) by the same procedure described in Intermediate 17 (reaction time: overnight). The title compound was obtained as a yellow oil (0.71 g, 76%) and used in the next step without further purification. MS (M+): 300.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178679B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-1638c158a15646ddacc84ae7562f4c19 |
| Source note | uspto-grants-2012_05 |